Comparison of different sample preparation techniques in TEM observation of microstructure of INCONEL alloy 783 subjected to prolonged isothermal exposure.

نویسنده

  • Longzhou Ma
چکیده

INCONEL alloy 783 was annealed and aged following the standard heat treatment procedure. One set of specimens was then isothermally exposed at 500 degrees C for 3000 h. Mechanical properties were measured at room temperature and 650 degrees C, and the results showed the prolonged exposure increased the strength and decreased elongation of alloy 783. The microstructures of as-produced and exposed material were examined using optical microscope, SEM and TEM, respectively. Three techniques, jet electro-polishing, ion milling, and focused ion beam, were employed to prepare the TEM samples to observe the variation of microstructure of alloy 783 due to isothermal exposure. TEM images of samples prepared by different methods were analyzed and compared. The results indicate that the jet electro-polishing technique allows the detail microstructure of alloy 783 subjected to different treatments to be well revealed, and thereby the TEM images can be used to explain the enhancement of strength of alloy 783 caused by isothermal exposure.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Transmission Electron Microscopy Sample Preparation of INCONEL 738 Nickel-Base Superalloy

Size, shape, volume fraction and distribution of embedded g/ phase in g phase has direct effect on strength of INCONEL alloy. Microstructure parameters of INCONEL phases are quantified from microstructure images using transmission electron microscopy (TEM). Different TEM sample preparation techniques were used to study INCONEL 738 alloy microstructure for transmission electron micros...

متن کامل

The effect of bonding temperature on the microstructure and mechanical properties of 939 super alloy by transient liquid phase bonding method

In this research, the effect of bonding temperature on the microstructure and mechanical properties of Inconel 939 super alloy by transient liquid phase bonding method. For this purpose, the middle layer of MBF20 with a thickness of 50 microns and three temperatures of 1060 °C, 1120 °C, 1180 °C and a time of 45 minutes have been used. In order to evaluate the microstructure, a scanning electron...

متن کامل

The effect of bonding temperature on the microstructure and mechanical properties of 939 super alloy by transient liquid phase bonding method

In this research, the effect of bonding temperature on the microstructure and mechanical properties of Inconel 939 super alloy by transient liquid phase bonding method. For this purpose, the middle layer of MBF20 with a thickness of 50 microns and three temperatures of 1060 °C, 1120 °C, 1180 °C and a time of 45 minutes have been used. In order to evaluate the microstructure, a scanning electron...

متن کامل

Investigation on the Effect of Post Weld Heat Treatment Temperature on Stress Corrosion Resistance of Inconel 625 Cladded on AISI 4130 Steel Using Hot Wire GTAW

In this research  the effect of heat treatment offer welding (PWHT) in 650,750 and 8500C for two hours on Sulfide stress corrosion cracking resistance (SSC), welding metal Inconel 625 to low alloy steel 4130 was analyzed that was welded using Automatic TIG welding process then the mechanical properties of the joint was observed using micro hardness measure experiment (weld metal, base metal and...

متن کامل

Investigation on the Effect of Post Weld Heat Treatment Temperature on Stress Corrosion Resistance of Inconel 625 Cladded on AISI 4130 Steel Using Hot Wire GTAW

In this research  the effect of heat treatment offer welding (PWHT) in 650,750 and 8500C for two hours on Sulfide stress corrosion cracking resistance (SSC), welding metal Inconel 625 to low alloy steel 4130 was analyzed that was welded using Automatic TIG welding process then the mechanical properties of the joint was observed using micro hardness measure experiment (weld metal, base metal and...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Micron

دوره 35 4  شماره 

صفحات  -

تاریخ انتشار 2004